SysGraph – Visualised thermal process safety
|Thermal analysis – Reaction calorimetry – Run-away scenario||Download Flyer|
|Don’t leave safety to chance|
As an integrated module, ThermoGraph provides thermokinetic analyses of all FlexyTSC applications such as RADEX and SEDEX.
Prognoses of thermal stability of chemical substances or reaction solutions right through to distillation residue all require precise calculation of the kinetics of possible decomposition reactions.
For storage and transportation tests, the kinetic properties of the various substances needs to be determined accurately. Thus, for example, the SADT (Self-Accelerating Decomposition Temperature) is determined to ensure safe transportation of chemical goods.
TMRadia24 is a further indicator to assess the criticality of processes.
Conventional measuring methods presuppose first order decomposition, which, however, is only rarely the case. Adiabatic analysis can provide information that is more accurate.
In addition to decomposition energy and onset temperature, ThermoGraph calculates the following indicators from only one adiabatic experiment:
All results are automatically corrected with phi and may therefore be directly included in the risk analysis.
Base lines can either be defined automatically by the evaluation software or custom created in the graphics interface.
Available for conventional isothermal reaction calorimetry as well as in combination with the Calo2310 pro for heat flow and heat balance evaluations.
Setting up safe processes also includes evaluation (risk analysis) of various influencing factors in order to minimise the thermal risks of a batch or semi-batch reaction.
KaloGraph visualises relevant results in a clear plot, for example:
The results mentioned above depend on the type of reaction control and can be determined for the reactor term as well as the reflux condenser.
You will recognise quickly and easily how strong a reaction accumulates and which criticality class a process has to be assigned to.
KaloGraph supports your optimisation processes with regard to economics, safety and kinetics.